Reaktion #53582

Reaktionsgleichung

[2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)phenyl]methyl sulfide

2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)thiophenol

→

2-chloro-4-fluoro-5-(3-trifluoromethyltriazolyl)benzene

Ausbeute 85.7%

Reaktionsbedingungen

Vorschrift

2.2 g (7.1 mmol) of [2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)phenyl]methyl sulfide was converted to 2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)thiophenol in the same manner as in Reference Example 1 and then to 1.8 g of 1,1′-thiodi-[2-chloro-4-fluoro-5-(3-trifluoromethyltriazolyl)benzene (yield 85.7%) in the same manner as in Reference Example (1), which was used in Example 2 (4) as the starting material.

Quelle