Reaktion #534053

ord-c83a4f0d57c74fe181a9d38a51e3f312

Reaktionsgleichung

O=C(O)c1ccc(S(=O)(=O)Nc2ccccc2C(=O)c2ccc(Cl)cc2Cl)cc1
4-[2-(2,4-dichloro-benzoyl)-phenylsulfamoyl]-benzoic acid
CCOC(=O)CN.Cl
glycine ethyl ester hydrochloride
→
CCOC(=O)CNC(=O)c1ccc(S(=O)(=O)Nc2ccccc2C(=O)c2ccc(Cl)cc2Cl)cc1
{4-[2-(2,4-Dichloro-benzoyl)-phenylsulfamoyl]-benzoylamino}-acetic acid ethyl ester
CCOC(=O)CNC(=O)c1ccc(S(=O)(=O)Nc2ccccc2C(=O)c2ccc(Cl)cc2Cl)cc1
title compound

Edukte

O=C(O)c1ccc(S(=O)(=O)Nc2ccccc2C(=O)c2ccc(Cl)cc2Cl)cc1
4-[2-(2,4-dichloro-benzoyl)-phenylsulfamoyl]-benzoic acid
CCOC(=O)CN.Cl
glycine ethyl ester hydrochloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 4-[2-(2,4-dichloro-benzoyl)-phenylsulfamoyl]-benzoic acid and glycine ethyl ester hydrochloride according to the method described in Example 1.1/d. MS (EI) 536.1 (MH+).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08481527B2uspto-grants-2013_07