Reaktion #534052

ord-9fc3a9a811a44b3794bd1460dc8f914d

Reaktionsgleichung

Nc1ccccc1C(=O)c1ccc(Cl)cc1Cl
(2-amino-phenyl)-(2,4-dichloro-phenyl)-methanone
O=C(O)c1ccc(S(=O)(=O)Cl)cc1
4-chlorosulfonyl-benzoic acid
→
O=C(O)c1ccc(S(=O)(=O)Nc2ccccc2C(=O)c2ccc(Cl)cc2Cl)cc1
title compound
O=C(O)c1ccc(S(=O)(=O)Nc2ccccc2C(=O)c2ccc(Cl)cc2Cl)cc1
4-[2-(2,4-Dichloro-benzoyl)-phenylsulfamoyl]-benzoic acid

Edukte

Nc1ccccc1C(=O)c1ccc(Cl)cc1Cl
(2-amino-phenyl)-(2,4-dichloro-phenyl)-methanone
O=C(O)c1ccc(S(=O)(=O)Cl)cc1
4-chlorosulfonyl-benzoic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from (2-amino-phenyl)-(2,4-dichloro-phenyl)-methanone [Synthesis, (1980) 677-688] and 4-chlorosulfonyl-benzoic acid according to the method described in Example 1.1/c. MS (EI) 451 (MH+).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08481527B2uspto-grants-2013_07