Reaktion #534042

ord-9f8f78fa473444929a643768433d05f1

Reaktionsgleichung

O=C(O)c1ccc(S(=O)(=O)Nc2ccccc2Oc2ccccc2)cc1
4-(2-phenoxy-phenylsulfamoyl)-benzoic acid
CCOC(=O)CN.Cl
glycine ethyl ester hydrochloride
→
CCOC(=O)CNC(=O)c1ccc(S(=O)(=O)Nc2ccccc2Oc2ccccc2)cc1
title compound
CCOC(=O)CNC(=O)c1ccc(S(=O)(=O)Nc2ccccc2Oc2ccccc2)cc1
[4-(2-Phenoxy-phenylsulfamoyl)-benzoylamino]-acetic acid ethyl ester

Edukte

O=C(O)c1ccc(S(=O)(=O)Nc2ccccc2Oc2ccccc2)cc1
4-(2-phenoxy-phenylsulfamoyl)-benzoic acid
CCOC(=O)CN.Cl
glycine ethyl ester hydrochloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 4-(2-phenoxy-phenylsulfamoyl)-benzoic acid and glycine ethyl ester hydrochloride (Aldrich) according to the method described in Example 1.1/d. MS (EI) 455.2 (MH+).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08481527B2uspto-grants-2013_07