Reaktion #530258

ord-389b46c53ae544379dc6a303293b1a5f

Reaktionsgleichung

CC(=O)OC(C(N)=O)C(C)c1ccccc1
carbamoyl-2-phenyl propanol acetate
CC(=O)OC[C@@H](CC(N)=O)c1ccccc1
(S)-3-carbamoyl-2-phenyl propanol acetate
→
CC(c1ccccc1)C(O)C(N)=O
carbamoyl-2-phenyl propanol

Edukte

CC(=O)OC(C(N)=O)C(C)c1ccccc1
carbamoyl-2-phenyl propanol acetate
CC(=O)OC[C@@H](CC(N)=O)c1ccccc1
(S)-3-carbamoyl-2-phenyl propanol acetate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Except for using (S)-3-N-morphoryl carbamoyl-2-phenyl propanol acetate, instead of (S)-3-carbamoyl-2-phenyl propanol acetate as the starting material, the same procedure with that of Example 38 was repeated.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05892088uspto-grants-1999_04