Reaktion #527809
ord-421b47c7408749a68881a84dac61fe1d
Reaktionsgleichung
ethanol
2-ethylhexylamine
2-(4-camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine
sodium acetate
→
2,4-Bis(2-ethyl-hexylamino)-6-(4-camphylidenemethylene-anilino)-1,3,5-triazine
Edukte
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeWhen the starting materials have reacted completely
Vorschrift
A reaction mixture comprising 33 g (0.26 mol) of 2-ethylhexylamine and 50 g (0.12 mol) of 2-(4-camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine in toluene is heated to 90° C. in the presence of sodium acetate. When the starting materials have reacted completely, the mixture is worked up. The product (95%) is a yellow viscous oil. UV (ethanol, c=1 mg/100 ml): λmax =345 nm, E=0.57.