Reaktion #523365

Reaktionsgleichung

sodium methoxide

2-methyl-3-furan thiol

chloromethyl methyl sulfide

→

(2-METHYL-3-FURYL)(METHYLTHIOMETHYL) SULFIDE

Lösungsmittel

methanol

methanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeInto a 25 ml round bottom flask equipped with magnetic stirrer
2. 2
   Temperaturthermometer, water bath, and reflux condenser
3. 3
   workup.ADDITIONis added a solution
4. 4
   TemperaturWhile maintaining the solution at 25° C-30° C
5. 5
   SonstigeAt 25° C

Vorschrift

Into a 25 ml round bottom flask equipped with magnetic stirrer, thermometer, water bath, and reflux condenser is added a solution containing 0.27 g of sodium methoxide (0.005 moles) in 3 ml. absolute methanol. While maintaining the solution at 25° C-30° C, 0.57 g (0.005 moles) of 2-methyl-3-furan thiol in 2 ml of absolute methanol is added thereto. At 25° C, 0.483 g (0.005 moles) of chloromethyl methyl sulfide having the formula:

Quelle