Reaktion #5223

ord-dcadfe0e1eca4e47a8b88dad58fe8309

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.STIRRINGThereafter, the mixture was stirred at room temperature for 19 hours

Vorschrift

2-Aminoethanol (13.76 g, 225.3 mmol) was dissolved in CHCl3 (750 ml). To the solution was added dropwise palmitoyl chloride (15.48 g, 56.3 mmol) with stirring under ice cooling. Thereafter, the mixture was stirred at room temperature for 19 hours.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05243035uspto-grants-1993_09