Reaktion #52203

Reaktionsgleichung

2,4-Dichlorobenzenesulphonyl chloride

1-propylamine

→

title compound

2,4-Dichloro-1-(1-propylsulphamoyl)benzene

Lösungsmittel

n-butanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturat reflux for 48 hour
2. 2
   SonstigeThe volatiles were removed by evaporation
3. 3
   Sonstigethe residue triturated with ether
4. 4
   Filtrationthe product collected by filtration

Vorschrift

2,4-Dichlorobenzenesulphonyl chloride (500 mg 2.1 mmol) and 1-propylamine (0.2 ml, 2.4 mmol) in n-butanol (10 ml) was heated at reflux for 48 hour. The volatiles were removed by evaporation and the residue triturated with ether and the product collected by filtration to give the title compound. NMR: 0.78 (t, 3H), 1.35 (q, 2H), 2.79 (t, 2H), 7.60 (dd, 1H), 7.84 (d, 1H), 7.92 (d, 2H)

Quelle