Reaktion #52045

ord-7cd71137c4cd4066b112bd4c66abb70d

Reaktionsgleichung

CC(C)Cn1cnc2cnc3ccccc3c21
1-isobutyl-1H-imidazo[4,5-c]quinoline
CC(=O)OO
peracetic acid
CC(C)C[N+]1([O-])C=Nc2cnc3ccccc3c21
1-isobutyl-1H-imidazo[4,5-c]quinoline N-oxide

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The oxidation of 1-isobutyl-1H-imidazo[4,5-c]quinoline produced in Example 3 is carried out in toluene at 40-45° C. using peracetic acid as oxidant to produce 1-isobutyl-1H-imidazo[4,5-c]quinoline N-oxide. The product is isolated by filtration after addition of a sodium sulfate solution and ammonium hydroxide.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06852861B2uspto-grants-2005_02