Reaktion #518320

ord-926ce0fb4e5e4ea99f38c6af10d7c527

Reaktionsgleichung

O=C(O)CS(=O)(=O)Cc1ccc(Cl)cc1
4-chlorobenzyl sulfonylacetic acid
O=Cc1ccc(Cl)cc1
4-chlorobenzaldehyde
→
O=S(=O)(/C=C/c1ccc(Cl)cc1)Cc1ccc(Cl)cc1
title compound
Ausbeute 80.0%
O=S(=O)(/C=C/c1ccc(Cl)cc1)Cc1ccc(Cl)cc1
(E)-4-chlorostyryl 4-chlorobenzyl sulfone
Ausbeute 80.0%

Edukte

O=C(O)CS(=O)(=O)Cc1ccc(Cl)cc1
4-chlorobenzyl sulfonylacetic acid
O=Cc1ccc(Cl)cc1
4-chlorobenzaldehyde

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

A solution of 4-chlorobenzyl sulfonylacetic acid (0.01 mol) and 4-chlorobenzaldehyde (0.01 mol) was subjected to Procedure 1, Part B. The title compound was obtained in 80% yield.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06656973B2uspto-grants-2003_12