Reaktion #518024

Reaktionsgleichung

N-butylidenebutylamine

ethyl diazoacetate

tetrahydrofuran

→

1-butyl-2-ethoxycarbonyl-3-propylaziridine

Ausbeute 45.0%

Reaktionsbedingungen

Vorschrift

A mixture of 0.5 mmol of N-butylidenebutylamine, 1 mmol of ethyl diazoacetate, 0.015 mmol of di-μ-chlorotetrakis(cyclooctene)diiridium(I) [Ir2Cl2(cyclooctene)4], and 0.5 ml of tetrahydrofuran was stirred at room temperature (25° C.) in an argon atmosphere for 3 hours to yield 1-butyl-2-ethoxycarbonyl-3-propylaziridine in a yield of 45%.

Quelle