Reaktion #518022

Reaktionsgleichung

N-butylidenebutylamine

ethyl diazoacetate

ethanol

→

1-butyl-2-ethoxycarbonyl-3-propylaziridine

Ausbeute 30.0%

Reaktionsbedingungen

Vorschrift

A mixture of 0.5 mmol of N-butylidenebutylamine, 0.5 mmol of ethyl diazoacetate, 0.015 mmol of di-μ-chlorotetrakis(cyclooctene)diiridium(I) [Ir2Cl2(cyclooctene)4] , and 0.5 ml of ethanol was stirred at room temperature (250° C.) in an argon atmosphere for 3 hours to yield 1-butyl-2-ethoxycarbonyl-3-propylaziridine in a yield of 30%.

Quelle