Reaktion #51739

Reaktionsgleichung

6-tert-butyl-4-thiocyanato-benzothiazol-2-yl-amine

dithiothreitol

phosphate

→

title compound

2-Amino-6-tert-butyl-benzothiazole-4-thiol

Lösungsmittel

EtOH

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe crude product was used further without any purification

Vorschrift

The title compound was prepared according to General Method 14 using 6-tert-butyl-4-thiocyanato-benzothiazol-2-yl-amine (Example L-6; 2.0 g. 7.6 mmol), dithiothreitol (4.6 g, 30 mmol), phosphate buffer of pH 7 (10 mL), and EtOH (50 mL). The crude product was used further without any purification. MS (APCI): 239 (M+H).

Quelle