Reaktion #51463

ord-d6bb0716c7774a2aab46372d086f0417

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeall volatiles were removed under reduced pressure

Vorschrift

N-Boc sarcosine piperonylamide (500 mg, 1.54 mmol) in methanol (10 mL) was treated with acetyl chloride (1 mL). After 45 minutes, all volatiles were removed under reduced pressure to yield sarcosine piperonyl amide hydrochloride (395 mg, quant.) as a sticky solid.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06849739B2uspto-grants-2005_02