Reaktion #51354

ord-2987ee0b3b8a42e0973ada939f899d39

Reaktionsgleichung

O=C(O)Cc1ccc(Cl)c(Cl)c1
3,4-dichlorophenylacetic acid
CCC(N)C(=O)OCC(C)C
iso-butyl 2-aminobutyrate
→
CCC(NC(=O)Cc1ccc(Cl)c(Cl)c1)C(=O)OCC(C)C
title compound
CCC(NC(=O)Cc1ccc(Cl)c(Cl)c1)C(=O)OCC(C)C
2-[(3,4-dichlorophenyl)acetamido]butyric acid iso-butyl ester

Edukte

O=C(O)Cc1ccc(Cl)c(Cl)c1
3,4-dichlorophenylacetic acid
CCC(N)C(=O)OCC(C)C
iso-butyl 2-aminobutyrate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Following General Procedure BI above and using 3,4-dichlorophenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure BJ above) the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06849650B2uspto-grants-2005_02