Reaktion #51342

Reaktionsgleichung

phenylacetyl chloride

D,L-alanine iso-butyl ester hydrochloride

→

title compound

N-(phenylacetyl)-D,L-alanine iso-butyl ester

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe reaction was monitored by tlc on silica gel and purification
2. 2
   Extraktionwas by extraction with Et2O

Vorschrift

Following General Procedure BA above and using phenylacetyl chloride (Aldrich) and D,L-alanine iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.

Quelle