Reaktion #51328

Reaktionsgleichung

2-aminonaphthalene

ethyl 2-bromobutyrate

→

title compound

2-[N-(naphth-2-yl)amino]butanoic acid ethyl ester

Lösungsmittel

CHCl3

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigePurification

Vorschrift

Following General Procedure AJ above and using 2-aminonaphthalene (Aldrich) and ethyl 2-bromobutyrate (Aldrich), the title compound was prepared as a solid, m.p. 81-83° C. The reaction was monitored by silica gel tlc (Rf=0.5 in CHCl3). Purification was by chromatography (silica gel using chloroform as the eluant).

Quelle