Reaktion #511491

Reaktionsgleichung

DIAD

4-hydroxy bromophenol

2-hydroxypropyl 2-methylacrylate

triphenyl phosphine

→

2-(4-bromophenoxy)propyl 2-methylacrylate

Lösungsmittel

THF

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethe same preparation procedure of Example 2
2. 2
   Sonstigeto give
3. 3
   Sonstigeafter chromatography purification pure 2-(4-bromophenoxy)propyl 2-methylacrylate as pale yellow oil

Vorschrift

Following the same preparation procedure of Example 2, the reaction was carried out with 4-hydroxy bromophenol (4 g), 2-hydroxypropyl 2-methylacrylate (3.33 g), triphenyl phosphine (6.06 g) and DIAD (4.69 g) in 50 ml of THF to give after chromatography purification pure 2-(4-bromophenoxy)propyl 2-methylacrylate as pale yellow oil.

Quelle