Reaktion #51078

Reaktionsgleichung

2-amino-3,5-dibromo-6-methylpyridine

1,1,3,3-tetramethylbutyl isocyanide

2,3-dimethoxybenzaldehyde

→

Compound ( 14 )

[6,8-dibromo-2-(2,3-dimethoxyphenyl)-5-methylimidazo[1,2-a]pyridin-3-yl]-(1,1,3,3-tetramethylbutyl)-amine

Lösungsmittel

perchloric acid

Reaktionsbedingungen

Vorschrift

Compound (14) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3,5-dibromo-6-methylpyridine solution (0.1 M, DCM), 0.575 ml of 1,1,3,3-tetramethylbutyl isocyanide solution (0.2 M, DCM), 0.500 ml of 2,3-dimethoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).

Quelle