Reaktion #50890

ord-873f2f7db5f04ea2a3c8c69096c5bc0a

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

U.S. Pat. No. 4,927,855 describes the preparation of the levorotatory enantiomer of modafinil by chiral resolution of the 2-[(diphenylmethyl)sulfinyl]acetic acid with α-methylbenzyl amine. After recovery and amidation of the enantiomerically pure acid, (−) modafinil was obtained as white crystals by crystallization from ethanol.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06849120B2uspto-grants-2005_02