Reaktion #507358

Reaktionsgleichung

n-pentane

tert-butyl fluoride

n-pentane

tert-butyl fluoride

→

Tert-Butyl Fluoride n-Pentane

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigekept at 0° C.
2. 2
   workup.ADDITIONwas poured in a glass
3. 3
   Sonstigealso kept at 0° C
4. 4
   workup.ADDITIONThe resulting solution was thoroughly mixed
5. 5
   Sonstigewas kept in the refrigerator at 0° C.

Vorschrift

500 mL of cold n-pentane kept at 0° C. was poured in a glass graduated cylinder. To the n-pentane was added 2.3 mL of tert-butyl fluoride also kept at 0° C. The resulting solution was thoroughly mixed and analyzed by CAP-GC by the CGSB method for gasoline. The concentration of the tert-butyl fluoride was found to be 0.43 wt %. The solution was kept in the refrigerator at 0° C.

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