Reaktion #50366

Reaktionsgleichung

glycidol

glycerin

p-hydroxy cinnamic acid

boron trifluoride ethyl ether

→

cinnamic acid

Lösungsmittel

DMSO

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturheating

Vorschrift

8.719 g of p-hydroxy cinnamic acid was dissolved in 10 ml of DMSO, and 19.7 g of glycidol was added. The mixture was stirred and heated to 90° C. Catalystic amount of boron trifluoride ethyl ether was added, heating and agitation was carried out for 2 hours and then the adduct of cinnamic acid and glycerin was obtained.

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