Reaktion #501848

Reaktionsgleichung

phenol

para-(methylthio)phenol

→

ortho(methylthio)phenol

Ausbeute 41.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   Filtrationfiltered
2. 2
   WaschenThe catalyst was washed several times with ether
3. 3
   Sonstigeto dry
4. 4
   Sonstigevolatiles were removed on a rotary flash evaporator

Vorschrift

The mixture was cooled to room temperature and filtered. The catalyst was washed several times with ether and allowed to dry. The filtrate and ether washings were combined, and volatiles were removed on a rotary flash evaporator. GC analysis indicated the presence of phenol (5.3 g. 42% recovered), ortho(methylthio)phenol (5.2 g. 41% yield), para-(methylthio)phenol (2.0 g, and di-(methylthio)phenols (2.0 g).

Quelle