Reaktion #49950

Reaktionsgleichung

N'-t-butyl-N'-(3-toluoyl)hydrazine

2-phenyl-3-methyl-pentanoyl chloride

→

N'-t-butyl-N-(2-phenyl-3-methylpentanoyl)-N'-(3-toluoyl)hydrazine

Lösungsmittel

toluene

—

hexanes

Reaktionsbedingungen

Aufarbeitung

1. 1
   Filtrationthe solids filtered
2. 2
   WaschenThe solids were washed with hexane and air
3. 3
   Sonstigedried

Vorschrift

To a stirred suspension of N'-t-butyl-N'-(3-toluoyl)hydrazine (0.7 g) in toluene (10 ml) and aqueous sodium hydroxide (12 drops of 50% aqueous sodium hydroxide) was added dropwise 2-phenyl-3-methyl-pentanoyl chloride (1.0 g). The reaction mixture was stirred overnight, diluted with hexanes and the solids filtered. The solids were washed with hexane and air dried.

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