Reaktion #49935

Reaktionsgleichung

N'-t-butyl-N-(2-furoyl)hydrazine

sodium hydroxide

benzoylchloride

→

N'-t-butyl-N-(2-furoyl)-N'-benzoylhydrazine

Lösungsmittel

toluene

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethe solid product, N'-t-butyl-N-(2-furoyl)-N'-benzoylhydrazine, was removed by filtration
2. 2
   Waschenwashed with water

Vorschrift

N'-t-butyl-N-(2-furoyl)hydrazine (1.0 g) was dissolved in 10 ml toluene and 2 ml water. 50% aqueous sodium hydroxide (1.0 g) was added followed by benzoylchloride (0.8 g). After stirring for 14 hours at room temperature, the solid product, N'-t-butyl-N-(2-furoyl)-N'-benzoylhydrazine, was removed by filtration and washed with water: m.p. 160°-162° C.

Quelle