Reaktion #49922

Reaktionsgleichung

N'-t-butyl-N-(2-pyridinecarbonyl)-hydrazine

sodium hydroxide

benzoyl chloride

→

N'-t-butyl-N-(2-pyridinecarbonyl)-N'-benzoylhydrazine

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe solids were removed by filtration
2. 2
   Waschenwashed with water

Vorschrift

A solution of N'-t-butyl-N-(2-pyridinecarbonyl)-hydrazine (1.0 g, 0.00518 mol) in 20 ml of toluene at 23° C. was treated sequentially with 50% sodium hydroxide (1.3 g) and benzoyl chloride (0.728 g). The mixture was stirred overnight. The solids were removed by filtration and washed with water to afford N'-t-butyl-N-(2-pyridinecarbonyl)-N'-benzoylhydrazine.

Quelle