Reaktion #499171

ord-d12fb8c7dd2a482b9551ddcb7e9bccb7

Reaktionsgleichung

O=C1CSCCN1Cc1ccc(Cl)c(Cl)c1
4-(3,4-dichlorobenzyl)-thiomorpholin-3-one
Clc1ccc(CBr)cc1Cl
3,4-dichlorobenzyl bromide
O=C1CSCCN1
thiomorpholin-3-one
→
O=C1CSCCN1Cc1ccccc1
4-Benzylthiomorpholin-3-one

Edukte

O=C1CSCCN1Cc1ccc(Cl)c(Cl)c1
4-(3,4-dichlorobenzyl)-thiomorpholin-3-one
Clc1ccc(CBr)cc1Cl
3,4-dichlorobenzyl bromide
O=C1CSCCN1
thiomorpholin-3-one

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

In the same manner, 4-(3,4-dichlorobenzyl)-thiomorpholin-3-one was prepared in 89% yield from 3,4-dichlorobenzyl bromide and thiomorpholin-3-one as a white solid.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06562813B2uspto-grants-2003_05