Reaktion #49707

Reaktionsgleichung

4'-n-octylbiphenyl-4-carboxylic acid

thionyl chloride

→

4'-n-octylbiphenyl-4-carboxylic acid chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturunder refluxing for 6 hours
2. 2
   workup.DISTILLATIONunaltered thionyl chloride was distilled off

Vorschrift

After 4'-n-octylbiphenyl-4-carboxylic acid (3.2 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours, unaltered thionyl chloride was distilled off to obtain 4'-n-octylbiphenyl-4-carboxylic acid chloride.

Quelle