Reaktion #49703

Reaktionsgleichung

4-n-octyloxybenzoic acid

thionyl chloride

→

4-n-octyloxybenzoic acid chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturunder refluxing for 6 hours
2. 2
   workup.DISTILLATIONunaltered thionyl chloride was distilled off

Vorschrift

After 4-n-octyloxybenzoic acid (11 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours, unaltered thionyl chloride was distilled off to obtain 4-n-octyloxybenzoic acid chloride.

Quelle