Reaktion #49702

Reaktionsgleichung

4-n-Hexyloxybiphenyl carboxylic acid

thionyl chloride

→

4-n-hexyloxybiphenyl carboxylic acid chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturunder refluxing for 6 hours
2. 2
   workup.DISTILLATIONUnaltered thionyl chloride was distilled off

Vorschrift

4-n-Hexyloxybiphenyl carboxylic acid (3.0 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours. Unaltered thionyl chloride was distilled off to obtain 4-n-hexyloxybiphenyl carboxylic acid chloride.

Quelle