Reaktion #49070

Reaktionsgleichung

D1

1-(dimethylamino)cyclopentanecarbonitrile

diethylamine hydrochloride

cyclopentanone

potassium cyanide

→

title compound

Ausbeute 62.0%

1-(Diethylamino)cyclopentanecarbonitrile

Ausbeute 62.0%

Lösungsmittel

water

Reaktionsbedingungen

Vorschrift

The title compound (2.06 g, 62%) was prepared from diethylamine hydrochloride (2.14 g, 20 mmol), cyclopentanone (1.68 g, 20 mmol) and potassium cyanide (1.30 g, 20 mmol) in water (10 ml) in a similar manner to that described in D1. 1H NMR (CDCl3) δ: 1.11 (6H, t, J=7 Hz), 1.78-1.88 (6H, m), 2.22 (2H, m), 2.71 (4H, q, J=7 Hz).

Quelle