Reaktion #488339
ord-c1928f7962f34a8f9a6d3e98261b013a
Reaktionsgleichung
Intermediate 12
2-(3,4-difluorophenyl)-1-phenylethanone
1,3-dibromobenzene
→
1-(3-bromophenyl)-2-phenylethanone
Ausbeute 47.7%
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1Sonstigewas purified by column chromatography (PE:EtOAc=100:1)
Vorschrift
Followed the procedure described in Intermediate 12, starting from 1,3-dibromobenzene, where the crude product was purified by column chromatography (PE:EtOAc=100:1) to give the desired 1-(3-bromophenyl)-2-phenylethanone (520 mg, yield 47.7%).