Reaktion #487529

ord-74aa5e5576d7455fa7be6743a8818c9c

Reaktionsgleichung

CCCCCC.CCOC(C)=O
Ethyl acetate Hexane
CCCCCCCC/C=C\CCCCCCCC(=O)Cl
Oleoyl chloride
C=CCCCCCCCCO
9-decen-1-ol
→
C=CCCCCCCCCOC(=O)CCCCCCC/C=C\CCCCCCCC
Compound F
Ausbeute 97.5%
C=CCCCCCCCCOC(=O)CCCCCCC/C=C\CCCCCCCC
Dec-9-enyl oleate
Ausbeute 97.5%

Edukte

CCCCCC.CCOC(C)=O
Ethyl acetate Hexane
CCCCCCCC/C=C\CCCCCCCC(=O)Cl
Oleoyl chloride
C=CCCCCCCCCO
9-decen-1-ol
—
compound F

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Compound F was prepared from Oleoyl chloride and 9-decen-1-ol following the general procedure already discussed and shown in FIG. 11. Pure compound F was a colorless oil obtained by column chromatography with Ethyl acetate/Hexane=1:40.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08741822B2uspto-grants-2014_06