Reaktion #482968

ord-4ae91a49d59f4d7ca3194e0b05198f68

Reaktionsgleichung

Nc1cccc(OCc2ccccc2)c1
3-benzyloxyaniline
CC(C)(C)c1ccc(-c2nc3ccc([N+](=O)[O-])cc3c(=O)o2)cc1
2-(4-tert-butylphenyl)-6-nitro-4H-3,1-benzoxazin-4-one
→
CC(C)(C)c1ccc(C(=O)Nc2ccc([N+](=O)[O-])cc2C(=O)Nc2cccc(OCc3ccccc3)c2)cc1
title compound
Ausbeute 42.0%
CC(C)(C)c1ccc(C(=O)Nc2ccc([N+](=O)[O-])cc2C(=O)Nc2cccc(OCc3ccccc3)c2)cc1
2-[(4-tert-Butylbenzoyl)amino]-N-(3-benzyloxyphenyl)-5-nitrobenzamide
Ausbeute 42.0%

Edukte

Nc1cccc(OCc2ccccc2)c1
3-benzyloxyaniline
CC(C)(C)c1ccc(-c2nc3ccc([N+](=O)[O-])cc3c(=O)o2)cc1
2-(4-tert-butylphenyl)-6-nitro-4H-3,1-benzoxazin-4-one

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using the procedure described in Example 91, Part B, 3-benzyloxyaniline (2.5 mmol) and 2-(4-tert-butylphenyl)-6-nitro-4H-3,1-benzoxazin-4-one (2.8 mmol) yielded 550 mg (42%) of the title compound.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06605626B2uspto-grants-2003_08