Reaktion #482946

ord-6bfbe3bb07cc4bca9bc0a354fbde3d3c

Reaktionsgleichung

Nc1cccc(OCc2ccccc2)c1
3-benzyloxyaniline
O=c1[nH]c2cc([N+](=O)[O-])ccc2c(=O)o1
4-nitroisatoic anhydride
→
Nc1cc([N+](=O)[O-])ccc1C(=O)Nc1cccc(OCc2ccccc2)c1
title product
Ausbeute 81.0%
Nc1cc([N+](=O)[O-])ccc1C(=O)Nc1cccc(OCc2ccccc2)c1
2-Amino-N-(3-benzyloxyphenyl)-4-nitrobenzamide
Ausbeute 81.0%

Edukte

Nc1cccc(OCc2ccccc2)c1
3-benzyloxyaniline
O=c1[nH]c2cc([N+](=O)[O-])ccc2c(=O)o1
4-nitroisatoic anhydride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using the procedure described in Example 91, Part B, 3-benzyloxyaniline (4.4 mmol) and 4-nitroisatoic anhydride (4.8 mmol) yielded 1.2 g (81%) of the title product.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06605626B2uspto-grants-2003_08