Reaktion #482626

ord-ed23711a5ad2474b9c67044e4d9050f5

Reaktionsgleichung

COc1cc(B(O)O)cc(OC)c1OC
3,4,5-Trimethoxyphenylboronic acid
CCOC(=O)c1cncc(Br)c1
ethyl 5-bromonicotinate
CCOC(=O)c1cncc(-c2cc(OC)c(OC)c(OC)c2)c1
title compound
CCOC(=O)c1cncc(-c2cc(OC)c(OC)c(OC)c2)c1
Ethyl 5-(3,4,5-Trimethoxyphenyl)nicotinate

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeas described in Preparation Example 1

Vorschrift

3,4,5-Trimethoxyphenylboronic acid (6.36 g) and ethyl 5-bromonicotinate (6.90 g) were reacted in the same manner as described in Preparation Example 1 to give the title compound.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06605620B1uspto-grants-2003_08