Reaktion #48151

ord-e154e83fd07f47c2b0a97803028e276e

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeIn analogy to the procedure described for the synthesis of example 6

Vorschrift

In analogy to the procedure described for the synthesis of example 6, the title compound was synthesized from (4,4-difluoro-piperidin-1-yl)-[5-(1-isopropyl-piperidin-4-yloxy)-1H-indol-2-yl]-methanone (intermediate 1) and 2-methoxy-5-pyrimidineboronic acid. The title compound was obtained in 9% yield as yellow oil. MS (m/e): 514.3 (MH+, 100%).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07745479B2uspto-grants-2010_06