Reaktion #480917

ord-ddacfc71a8504682a05627c6e4b3745c

Reaktionsgleichung

COC(=O)C1(CI)CCOCC1
4-iodomethyltetrahydropyran-4-carboxylic acid methyl ester
COC(=O)C1CCCCC1
cyclohexane-carboxylic acid methyl ester
→
COC(=O)C1(CI)CCCCC1
title compound
Ausbeute 100.0%
COC(=O)C1(CI)CCCCC1
1-Iodomethylcyclohexanecarboxylic acid methyl ester
Ausbeute 100.0%

Edukte

COC(=O)C1(CI)CCOCC1
4-iodomethyltetrahydropyran-4-carboxylic acid methyl ester
COC(=O)C1CCCCC1
cyclohexane-carboxylic acid methyl ester

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigePrepared

Vorschrift

Prepared according to the method for the preparation of 4-iodomethyltetrahydropyran-4-carboxylic acid methyl ester, from cyclohexane-carboxylic acid methyl ester (10 ml), to give the title compound as a brown gum (20 g, 100%).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06809100B2uspto-grants-2004_10