Reaktion #480673

ord-66014354b5374ffb9843a12927174c8f

Reaktionsgleichung

COC(=O)C1(CCCCBr)CCC1
1-(4-bromobutyl)cyclobutane carboxylic acid methyl ester
CS.[Na]
sodium methylmercaptan
→
COC(=O)C1(CCCCSC)CCC1
1-[4-(Methylthio)butyl]cyclobutane carboxylic acid methyl ester

Edukte

COC(=O)C1(CCCCBr)CCC1
1-(4-bromobutyl)cyclobutane carboxylic acid methyl ester
CS.[Na]
sodium methylmercaptan

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

1-[4-(Methylthio)butyl]cyclobutane carboxylic acid methyl ester was prepared from 1-(4-bromobutyl)cyclobutane carboxylic acid methyl ester and sodium methylmercaptan using the procedure described in example 172.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06806365B2uspto-grants-2004_10