Reaktion #476836

ord-e82cb9c16d524ad382d59b2d011bdb18

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigesuch in the next reaction step
  2. 2
    Sonstigewithout purification by chromatography

Vorschrift

Phenyl-methanethiol (4.g g, 37.0 mmol) was treated with commercially available 1-bromo-3-fluoro-2-trifluoromethyl-benzene (10.0 g, 41.1 mmol) in close analogy to the procedure described in step 5.3). The crude product (10.5 g) after workup was used as such in the next reaction step without purification by chromatography.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08378092B2uspto-grants-2013_02