Reaktion #476184

Reaktionsgleichung

8-chloro-1-octanol

2-hydroxy biphenyl

sodium iodide

sodium hydroxide

→

8-(biphenyl-2-yloxy)-octan-1-ol

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe compound was prepared
2. 2
   workup.ADDITIONwas added
3. 3
   SonstigeThe product was recovered essentially as in Preparatory Example 1

Vorschrift

The compound was prepared using essentially the procedure of Preparatory Example 1 with 2-hydroxy biphenyl (40 g.), water (250 g.), sodium iodide (3.5 g.) and sodium hydroxide (37.6 g. of 50% in water). This mixture was heated to 100° C. with agitation and 8-chloro-1-octanol (77.4 g.) was added. The product was recovered essentially as in Preparatory Example 1.

Quelle