Reaktion #474331

ord-26dc5fa6a64f467d96bf1c2da6a62b6f

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstige132 mg (94%) of target compound was obtained

Vorschrift

132 mg (94%) of target compound was obtained by using a method same as in Example 1 by using 3-(1-phenyl-3-propyl-1H-pyrazol-5-yl)propanal (75 mg, 0.310 mmol), 2-methyl-1-m-tolylpiperazine (59 mg, 0.310 mmol), DIPEA (0.081 mL, 0.465 mmol) and NaBH(OAc)3 (197 mg, 0.930 mmol).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08372844B2uspto-grants-2013_02