Reaktion #4741

ord-ab50ca1c8ca943ada3827a0b5fa3b8c3

Reaktionsgleichung

NC(=O)NNC(=O)NCCCOc1cccc(CN2CCCCC2)c1
N-[3-[3-(1-piperidinylmethyl) phenoxy]propyl]-1,2-hydrazine dicarboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride
→
Nc1nnc(NCCCOc2cccc(CN3CCCCC3)c2)o1
N-[3-[3-(1-Piperidinylmethyl)phenoxy]propyl]-1,3,4-oxadiazole-2,5-diamine

Edukte

NC(=O)NNC(=O)NCCCOc1cccc(CN2CCCCC2)c1
N-[3-[3-(1-piperidinylmethyl) phenoxy]propyl]-1,2-hydrazine dicarboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The compound is prepared by a method analogous to that of Example 40 from N-[3-[3-(1-piperidinylmethyl) phenoxy]propyl]-1,2-hydrazine dicarboxamide and phosphorus oxychloride.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04727081uspto-grants-1988_02