Reaktion #4731

ord-f89ec35a77d24dec965a72076856b42d

Reaktionsgleichung

O=C(NCCCOc1cccc(CN2CCCCC2)c1)NNC(=O)Nc1ccc(Cl)cc1
N-4-chlorophenyl-N'-[3-[3-(1piperidinylmethyl)phenoxy]propyl]-1,2-hydrazine dicarboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride
→
Clc1ccc(Nc2nnc(NCCCOc3cccc(CN4CCCCC4)c3)o2)cc1
N-4-Chlorophenyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-1,3,4-oxadiazole-2,5-diamine

Edukte

O=C(NCCCOc1cccc(CN2CCCCC2)c1)NNC(=O)Nc1ccc(Cl)cc1
N-4-chlorophenyl-N'-[3-[3-(1piperidinylmethyl)phenoxy]propyl]-1,2-hydrazine dicarboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The compound is prepared by a method analogous to that of Example 40 from N-4-chlorophenyl-N'-[3-[3-(1piperidinylmethyl)phenoxy]propyl]-1,2-hydrazine dicarboxamide and phosphorus oxychloride. The analytical values are summarized in Table III.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04727081uspto-grants-1988_02