Reaktion #4726

ord-d78e7903616a47b5a9621809086959ae

Reaktionsgleichung

CCCCNC(=O)NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1
N-butyl-2-[[3-[3-(1-piperidinylmethyl)phenoxy]propyl]aminothioxomethyl]hydrazine carboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride
→
CCCCNc1nnc(NCCCOc2cccc(CN3CCCCC3)c2)s1
N-Butyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]1,3,4-thiadiazole-2,5-diamine

Edukte

CCCCNC(=O)NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1
N-butyl-2-[[3-[3-(1-piperidinylmethyl)phenoxy]propyl]aminothioxomethyl]hydrazine carboxamide
O=P(Cl)(Cl)Cl
phosphorus oxychloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The compound is prepared by a method analogous to that of Example 40 from N-butyl-2-[[3-[3-(1-piperidinylmethyl)phenoxy]propyl]aminothioxomethyl]hydrazine carboxamide and phosphorus oxychloride. The analytical values are summarized in Table III.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04727081uspto-grants-1988_02