Reaktion #471780

Reaktionsgleichung

3-Aminopropyltriethoxysilane

6-(4-methoxy-benzoyl)-7-oxa-bicyclo[4.2.0]octan-8-one

→

title compound

2-Hydroxy-2-(4-methoxybenzoyl)cyclohexanecarboxylic acid(3-silanyl-propyl)-amide

Lösungsmittel

methylene chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   TemperaturThe reaction mixture is heated
2. 2
   Temperaturat reflux for several hours
3. 3
   SonstigeUpon completion of the reaction, solvent
4. 4
   Sonstigeis evaporated

Vorschrift

3-Aminopropyltriethoxysilane (22.14 g, 0.100 mol) is added to a solution of 26.03 g (0.100 mol) of 6-(4-methoxy-benzoyl)-7-oxa-bicyclo[4.2.0]octan-8-one in methylene chloride. The reaction mixture is heated at reflux for several hours and monitored by thin layer chromatography. Upon completion of the reaction, solvent is evaporated to obtain the title compound.

Quelle