Reaktion #470367

Reaktionsgleichung

Methoxymethylpyrrolidine

dimethyl carbonate

→

desired product

Ausbeute 60.0%

N-Methoxymethyl-N-Methylpyrrolidinium Methyl carbonate

Ausbeute 60.0%

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigereacted at 120° C. for 24 hours
2. 2
   FiltrationThe resulting solids were filtered off
3. 3
   Waschenwashed with dimethyl carbonate
4. 4
   SonstigeThe solids were dried in a vacuum

Vorschrift

Methoxymethylpyrrolidine (10.00 g) and 117.39 g of dimethyl carbonate were placed into an autoclave and reacted at 120° C. for 24 hours. The resulting solids were filtered off and washed with dimethyl carbonate. The solids were dried in a vacuum, giving 10.70 g of the desired product.

Quelle