Reaktion #470246
ord-c9efbc9b39db4d63a3aea5f0da4e858a
Reaktionsgleichung
4-Amino-3-methylbenzoic acid
N-BOC-4-aminobenzoic acid
→
desired product
N-BOC-4-Amino-3-methylbenzoic acid
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeThe resulting orange-brown solid was recrystallized from ethyl acetate and hexanes
Vorschrift
4-Amino-3-methylbenzoic acid (5 g, 33.1 mmol) was reacted according to the same procedure as that used in the process for preparing N-BOC-4-aminobenzoic acid. The resulting orange-brown solid was recrystallized from ethyl acetate and hexanes to provide the desired product (4.99 g) as tan prismatic crystals: m.p. 180-182° C.;