Reaktion #466928

ord-e5a6a6ef094a48d3b59b532b88ee6eec

Reaktionsgleichung

CCOC(=O)n1c(C(=O)c2ccc(F)cc2)c(NC(C)=O)c2ccc(Cl)cc21
3-acetylamino-6-chloro-1-ethoxycarbonyl-2-(4-fluorobenzoyl)indole
CCOC(=O)n1c(C(=O)c2ccc(F)cc2)c(NC(C)=O)c2ccc(Cl)cc21
3-Acetylamino-6-chloro-1-ethoxycarbonyl-2-(4-fluorobenzoyl)indole
→
CC(=O)Nc1c(C(=O)c2ccc(F)cc2)[nH]c2cc(Cl)ccc12
title compound
CC(=O)Nc1c(C(=O)c2ccc(F)cc2)[nH]c2cc(Cl)ccc12
3-Acetylamino-6-chloro-2-(4-fluorobenzoyl)indole

Edukte

CCOC(=O)n1c(C(=O)c2ccc(F)cc2)c(NC(C)=O)c2ccc(Cl)cc21
3-acetylamino-6-chloro-1-ethoxycarbonyl-2-(4-fluorobenzoyl)indole
CCOC(=O)n1c(C(=O)c2ccc(F)cc2)c(NC(C)=O)c2ccc(Cl)cc21
3-Acetylamino-6-chloro-1-ethoxycarbonyl-2-(4-fluorobenzoyl)indole

Reagenzien

Keine

Lösungsmittel

CCCCCC.CCO
ethanol hexane

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared according to the procedure described in step 2 of Example 2 (Method A) from 3-acetylamino-6-chloro-1-ethoxycarbonyl-2-(4-fluorobenzoyl)indole (step 1). m.p.: 205-207° C. (ethanol/hexane)

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06300363B1uspto-grants-2001_10